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MassMS-NW-3723 chlorodiphenylphosphine C12H10ClP (Mass of molecular ion: 220)
Source Temperature: 270 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 2.2 39.0 5.0 50.0 5.5 51.0 18.6 52.0 1.5 56.0 2.4 57.0 4.5 63.0 3.1 65.0 1.6 68.0 1.1 69.0 1.3 74.0 1.9 75.0 1.7 76.0 1.9 77.0 10.9 78.0 1.7 80.0 2.8 81.0 5.2 82.0 1.7 83.0 1.3 91.0 2.0 91.5 1.8 92.0 5.0 102.0 1.0 107.0 29.3 108.0 12.8 109.0 1.4 115.0 3.1 128.0 1.4 133.0 2.4 139.0 1.6 141.0 1.3 143.0 29.4 144.0 2.3 145.0 9.7 151.0 1.2 152.0 8.4 153.0 6.3 154.0 100.0 155.0 13.3 157.0 3.4 170.0 2.1 181.0 1.4 183.0 51.9 184.0 20.5 185.0 18.9 186.0 3.5 219.0 11.3 220.0 90.2 221.0 15.4 222.0 30.1 223.0 4.0 235.0 1.3 264.0 1.7 266.0 1.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H10 Cl P 0.04 ml : 0.5 ml CDCl3 chlorodiphenylphosphine 
Assign. Shift(ppm)
A 7.57 B 7.47 to 7.25
Hz ppm Int.687.69 7.679 148 685.94 7.660 127 685.44 7.654 140 684.56 7.644 188 683.75 7.635 153 683.25 7.629 142 682.19 7.618 201 680.81 7.602 311 679.44 7.587 233 678.00 7.571 485 677.00 7.560 298 676.13 7.550 261 674.13 7.528 355 673.19 7.517 312 671.50 7.498 277 670.31 7.485 416 668.69 7.467 236 666.44 7.442 208 664.44 7.419 349 662.88 7.402 757 661.50 7.387 1000 659.88 7.369 727 658.63 7.355 812 656.44 7.330 608 654.81 7.312 414 652.69 7.288 113
in CDCl3
liquid film
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