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2-Chloro-N,N-diethylacetamide

Product Name 2-Chloro-N,N-diethylacetamide

CAS2315-36-8

MFC6H12ClNO

MW149.62

¹³CNMR

Mass

MS-NW-1291          
N,N-diethylchloroacetamide
C6H12ClNO           (Mass of molecular ion:    149)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      14.0       1.2
      15.0       5.0
      18.0       2.3
      26.0       1.8
      27.0      13.0
      28.0       9.4
      29.0      30.8
      30.0      14.4
      41.0       3.4
      42.0      13.7
      43.0       3.5
      44.0      18.3
      49.0       7.3
      51.0       2.3
      56.0       6.9
      57.0       1.7
      58.0     100.0
      59.0       3.7
      70.0       1.3
      71.0       1.8
      72.0      42.9
      73.0       1.7
      77.0       6.6
      79.0       2.2
      86.0       1.2
     100.0      20.4
     101.0       1.2
     106.0       4.8
     108.0       1.7
     114.0      54.1
     115.0       4.1
     134.0      12.9
     136.0       4.2
     149.0      10.8
     151.0       3.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₂ Cl N O	0.04 ml : 0.5 ml CDCl₃
N,N-diethylchloroacetamide

    Assign.     Shift(ppm)

      A             4.070
      B     *1      3.397
      C     *1      3.383
      D     *2      1.241
      E     *2      1.159

     Hz     ppm     Int.

    364.50   4.070   1000
    315.00   3.518     50
    313.88   3.505     53
    307.88   3.438    158
    306.69   3.425    165
    300.81   3.359    169
    299.56   3.345    170
    293.75   3.280     58
    292.38   3.265     60
    118.31   1.322    151
    111.25   1.243    310
    109.88   1.227    205
    106.75   1.192     32
    103.94   1.161    167
    102.69   1.147    317
     95.56   1.067    126

in CDCl3

CCl4 solution

liquid film

4880 A,200 M,liquid

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