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WebSite > CAS DataBase List >  22856-62-8More Spectrum > 4,4'-DIAMINO-2,2'-DIMETHYLBIBENZYL(22856-62-8)IR2

22856-62-8

4,4'-DIAMINO-2,2'-DIMETHYLBIBENZYL

Product Name 4,4'-DIAMINO-2,2'-DIMETHYLBIBENZYL

CAS22856-62-8

MFC16H20N2

MW240.34

  • 22856-62-8_ms_1
    Mass

    MS-NW-8079          
    4,4'-ethylenedi(m-toluidine)
    C16H20N2            (Mass of molecular ion:    240)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       1.2
          77.0       3.3
          91.0       2.2
          93.0       1.3
         103.0       1.4
         118.0       1.3
         119.0       1.8
         120.0     100.0
         121.0       9.5
         148.0       1.4
         240.0      12.3
         241.0       2.3
    

400 MHz in DMSO-d6

  • 22856-62-8_1hnmr_1

    1H NMR 399.65 MHz
    C16 H20 N2 0.033 g : 0.5 ml DMSO-d6
    4,4'-ethylenedi(m-toluidine)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.772 B 6.358 C 6.330 D 4.71 E 2.517 F 2.108 J(A,C)=7.9HZ J(B,C)=2.2HZ

         Hz     ppm     Int.
    

       2710.57   6.783    199
       2702.64   6.763    212
       2542.11   6.361    187
       2540.16   6.356    248
       2534.67   6.343    158
       2532.35   6.337     99
       2526.86   6.323    128
       2524.41   6.317     97
       1883.42   4.713    382
       1005.86   2.517    654
        855.47   2.141     21
        854.74   2.139     23
        854.37   2.138     24
        842.53   2.109   1000
    

in DMSO-d6

in CDCl3

  • 22856-62-8_13cnmr_1

  • 22856-62-8_13cnmr_2

KBr disc

  • 22856-62-8_ir1_2

nujol mull

  • 22856-62-8_ir2_1

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