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MS-IW-1274 p-propylaniline C9H13N (Mass of molecular ion: 135)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
39.0 1.5 51.0 1.4 52.0 1.2 53.0 1.1 65.0 2.2 77.0 6.0 78.0 2.4 79.0 4.0 91.0 1.4 92.0 1.4 93.0 1.3 104.0 1.2 106.0 100.0 107.0 8.7 118.0 1.1 119.0 1.2 135.0 26.7 136.0 2.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N 0.05 ml : 0.5 ml CDCl3 p-propylaniline Assign. Shift(ppm)
A 6.936 B 6.563 C 3.41 D 2.453 E 1.562 F 0.902
Hz ppm Int.
2779.30 6.955 49 2776.73 6.948 389 2774.66 6.943 142 2770.39 6.933 149 2768.19 6.927 470 2766.24 6.922 57 2765.63 6.921 67 2628.66 6.578 67 2626.10 6.572 506 2623.90 6.566 182 2619.63 6.555 166 2617.55 6.550 512 2614.99 6.544 64 1363.77 3.413 42 988.53 2.474 229 980.96 2.455 299 973.14 2.435 264 644.04 1.612 50 636.60 1.593 183 629.03 1.574 273 622.80 1.559 122 621.58 1.556 301 615.60 1.541 53 614.01 1.537 199 606.81 1.519 57 367.92 0.921 543 360.60 0.903 1000 353.27 0.884 532
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