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MassMS-NW-5217 methyl 1-naphthyl ether C11H10O (Mass of molecular ion: 158)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.6 28.0 1.1 39.0 4.3 50.0 2.7 51.0 3.4 62.0 3.5 63.0 8.1 64.0 1.5 65.0 4.1 74.0 3.0 75.0 3.7 76.0 1.5 77.0 2.7 79.0 2.4 86.0 1.5 87.0 2.1 88.0 2.2 89.0 6.8 101.0 1.4 113.0 2.4 114.0 4.0 115.0 79.7 116.0 8.1 126.0 2.7 127.0 5.4 128.0 4.9 129.0 2.2 143.0 35.6 144.0 4.3 157.0 2.0 158.0 100.0 159.0 11.7
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C11 H10 O 0.031 g : 0.5 ml CDCl3 methyl 1-naphthyl ether 
Assign. Shift(ppm)
A 8.260 B 7.765 C 7.59 to 7.31 D 6.776 E 3.963
Hz ppm Int.744.88 8.318 35 744.31 8.311 48 741.75 8.283 31 740.44 8.268 32 738.25 8.244 55 735.13 8.209 43 734.50 8.202 58 701.94 7.838 39 701.25 7.830 40 698.38 7.798 61 696.25 7.775 47 694.44 7.754 51 692.31 7.731 75 691.63 7.723 70 675.75 7.546 32 675.19 7.539 30 672.06 7.505 208 669.06 7.471 110 668.44 7.464 108 666.13 7.438 85 665.31 7.429 100 663.00 7.403 302 662.44 7.397 195 660.50 7.375 105 660.06 7.371 102 658.56 7.354 35 657.38 7.341 189 611.19 6.825 70 608.19 6.791 48 605.38 6.760 54 602.44 6.727 52 355.06 3.965 1000 354.75 3.962 999
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1H NMR 399.65 MHz C11 H10 O 0.031 g : 0.5 ml CDCl3 methyl 1-naphthyl ether Assign. Shift(ppm)
A 8.263 B 7.742 C *1 7.43 D *1 7.43 E 7.372 F 7.309 G 6.694 J 3.863 J(F,G)=7.3HZ. J(E,G)=1.0HZ.
Hz ppm Int.3307.62 8.277 50 3306.88 8.275 83 3306.15 8.273 55 3304.69 8.269 43 3303.71 8.267 44 3303.10 8.265 48 3302.37 8.264 47 3300.90 8.260 69 3300.17 8.258 71 3297.85 8.252 52 3297.12 8.251 84 3296.39 8.249 53 3098.88 7.754 75 3095.70 7.747 89 3093.38 7.741 61 3092.04 7.737 50 3091.67 7.736 51 3089.36 7.731 83 2976.68 7.449 45 2975.95 7.447 40 2972.78 7.439 286 2969.85 7.432 149 2969.12 7.430 147 2966.92 7.424 136 2965.94 7.422 133 2963.13 7.415 259 2960.08 7.407 30 2959.11 7.405 35 2952.03 7.387 63 2951.29 7.385 87 2943.73 7.366 113 2942.99 7.364 148 2927.49 7.326 167 2919.92 7.307 175 2919.19 7.305 114 2911.62 7.286 99 2679.44 6.705 113 2678.59 6.703 113 2671.88 6.686 105 2671.02 6.684 104 1543.82 3.863 1000
in CDCl3
liquid film
4880 A,200 M,liquid
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