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MS-NW-6772 di(methyl-d3) sulfoxide C2D6OS (Mass of molecular ion: 84)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
16.0 1.7 18.0 14.2 28.0 2.0 30.0 4.3 32.0 1.3 34.0 7.5 36.0 3.3 38.0 4.9 44.0 1.2 46.0 14.4 48.0 9.2 50.0 7.8 52.0 2.3 64.0 3.2 66.0 100.0 67.0 2.0 68.0 5.2 84.0 84.5 85.0 2.5 86.0 4.2
90 MHz in CDCl3
Neat
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1H NMR 89.56 MHz C2 D6 O S 0.05 ml : 0.5 ml CDCl3 di(methyl-d3) sulfoxide Assign. Shift(ppm)
A 2.59 J(H,D)=-1.7HZ
Hz ppm Int.
239.75 2.677 62 239.38 2.673 62 238.38 2.662 60 237.94 2.657 71 237.06 2.647 123 235.63 2.631 391 233.75 2.610 722 231.81 2.589 1000 230.00 2.569 715 228.19 2.548 370 226.56 2.530 92 226.06 2.525 69 224.38 2.506 65
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