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MassMS-IW-4862 4,4'-ethylidenediphenol C14H14O2 (Mass of molecular ion: 214)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 1.4 51.0 1.0 55.0 2.9 63.0 1.0 65.0 1.9 76.0 1.8 77.0 2.5 84.0 1.1 90.0 1.6 90.5 2.0 91.0 3.0 99.0 2.2 99.5 4.1 103.0 1.2 107.0 3.1 115.0 1.7 119.0 2.1 120.0 2.6 121.0 3.2 128.0 1.2 131.0 1.2 141.0 1.3 152.0 2.8 153.0 2.2 169.0 2.1 170.0 1.5 181.0 5.6 182.0 1.4 197.0 3.2 198.0 2.9 199.0 100.0 200.0 14.4 201.0 1.3 213.0 2.0 214.0 39.2 215.0 6.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C14 H14 O2 0.039 g : 0.5 ml DMSO-d6 4,4'-ethylidenediphenol 
Assign. Shift(ppm)
A 9.14 B 7.001 C 6.666 D 3.912 E 1.462
Hz ppm Int.3653.11 9.141 1000 2805.18 7.020 67 2802.43 7.013 476 2800.60 7.008 172 2795.87 6.996 191 2794.04 6.992 547 2791.14 6.984 72 2671.20 6.684 84 2668.30 6.677 644 2666.17 6.672 199 2661.74 6.661 199 2659.76 6.656 570 2656.71 6.648 68 1574.86 3.941 23 1567.69 3.923 78 1560.52 3.905 80 1553.34 3.887 25 587.92 1.472 362 580.75 1.454 359
in CDCl3
KBr disc
nujol mull
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