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Diethyl azodicarboxylate

Product Name Diethyl azodicarboxylate

CAS1972-28-7

MFC6H10N2O4

MW174.15

¹³CNMR

Mass

MS-NW-1286          
diethyl azodiformate
C6H10N2O4           (Mass of molecular ion:    174)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       2.2
      26.0       1.1
      27.0      15.0
      28.0      20.4
      29.0     100.0
      30.0       2.2
      31.0       2.2
      32.0       4.4
      43.0       1.6
      44.0       1.1
      45.0       2.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₁₀ N₂ O₄	0.04 ml : 0.5 ml CDCl₃
diethyl azodiformate

    Assign.     Shift(ppm)

      A             4.505
      B             1.444

     Hz     ppm     Int.

    414.56   4.629    125
    407.25   4.548    427
    400.13   4.468    445
    393.13   4.390    145
    136.25   1.522    465
    129.19   1.443   1000
    122.00   1.363    414

in CDCl3

CCl4 solution

liquid film

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