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MS-NW-1553 methyl m-hydroxybenzoate C8H8O3 (Mass of molecular ion: 152)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 5.6 27.0 1.0 29.0 2.7 37.0 1.8 38.0 5.7 39.0 22.5 50.0 2.7 51.0 1.9 53.0 4.5 59.0 1.1 61.0 1.8 62.0 4.2 63.0 11.6 64.0 6.9 65.0 33.2 66.0 3.1 74.0 1.6 75.0 1.2 92.0 4.8 93.0 41.8 94.0 4.8 95.0 1.5 107.0 1.4 121.0 100.0 122.0 8.3 123.0 1.0 152.0 49.2 153.0 4.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H8 O3 0.041 g : 0.5 ml CDCl3 methyl m-hydroxybenzoate Assign. Shift(ppm)
A 7.61 B 7.60 C 7.300 D 7.089 E 6.31 F 3.918
Hz ppm Int.
684.63 7.645 75 683.69 7.634 98 682.06 7.616 81 681.25 7.607 88 679.63 7.589 84 678.31 7.574 75 676.88 7.558 111 675.38 7.542 43 662.06 7.393 63 654.06 7.304 127 646.25 7.216 72 639.31 7.139 57 637.81 7.122 64 636.81 7.111 54 635.38 7.095 53 567.06 6.332 43 564.31 6.301 83 350.88 3.918 1000
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