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MassMS-IW-2619 1-bromopyrene C16H9Br (Mass of molecular ion: 280)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
74.0 2.3 75.0 1.3 86.0 1.3 87.0 5.8 87.5 1.3 98.0 1.5 99.0 6.9 99.5 6.4 100.0 34.6 100.5 21.0 101.0 3.4 140.0 12.2 140.5 2.3 141.0 12.1 141.5 2.1 150.0 2.0 151.0 1.2 174.0 3.0 175.0 2.3 198.0 5.6 199.0 7.6 200.0 39.0 201.0 52.4 202.0 9.2 280.0 100.0 281.0 18.2 282.0 98.2 283.0 17.2 284.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H9 Br 0.033 g : 0.5 ml CDCl3 1-bromopyrene 
Assign. Shift(ppm)
A 8.350 B 8.16 C 8.14 D 8.077 E *1 8.00 F 7.98 G *1 7.925 J 7.911 ASSIGNED BY C-H COSY.
Hz ppm Int.3342.16 8.363 487 3333.01 8.340 575 3264.53 8.169 654 3258.06 8.153 339 3256.35 8.149 1000 3250.73 8.134 435 3249.02 8.130 448 3232.42 8.089 520 3223.14 8.065 444 3202.03 8.013 350 3193.24 7.991 690 3188.84 7.980 36 3186.28 7.973 529 3178.59 7.954 281 3170.41 7.933 594 3165.53 7.921 483 3161.50 7.911 351 3157.35 7.901 419
in CDCl3
KBr disc
nujol mull
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