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MassMS-NW-7595 2,3-epoxypinane C10H16O (Mass of molecular ion: 152)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.3 17.0 1.2 18.0 5.1 27.0 15.7 28.0 1.9 29.0 8.5 38.0 1.7 39.0 27.2 40.0 5.2 41.0 51.7 42.0 4.0 43.0 14.5 50.0 2.9 51.0 9.2 52.0 4.0 53.0 17.3 54.0 5.7 55.0 45.1 56.0 4.9 57.0 1.6 58.0 1.2 62.0 1.3 63.0 3.9 64.0 1.6 65.0 10.9 66.0 14.7 67.0 48.1 68.0 8.7 69.0 33.2 70.0 4.4 71.0 1.0 77.0 21.1 78.0 6.5 79.0 18.7 80.0 4.5 81.0 27.8 82.0 13.3 83.0 39.0 84.0 4.6 89.0 1.3 91.0 43.4 92.0 16.6 93.0 68.4 94.0 10.2 95.0 43.8 96.0 7.2 97.0 6.4 98.0 1.2 103.0 3.2 104.0 1.9 105.0 9.6 106.0 4.3 107.0 8.9 108.0 100.0 109.0 37.8 110.0 8.6 111.0 3.8 115.0 4.3 116.0 1.4 117.0 8.6 118.0 1.4 119.0 39.6 120.0 4.2 121.0 2.4 123.0 2.4 131.0 1.3 132.0 5.5 133.0 1.9 134.0 14.5 135.0 2.7 136.0 1.0 137.0 12.5 138.0 1.4 152.0 7.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H16 O 0.05 ml : 0.5 ml CDCl3 2,3-epoxypinane 
Assign. Shift(ppm)
A 3.066 B 2.00 C 1.98 D 1.947 E 1.911 F 1.73 G 1.623 J *1 1.342 K *1 1.294 L *1 0.944
Hz ppm Int.1228.15 3.074 108 1226.93 3.071 113 1224.00 3.063 111 1222.78 3.060 112 811.77 2.032 70 808.59 2.024 80 803.83 2.012 64 802.00 2.007 70 800.54 2.004 46 798.58 1.999 56 796.51 1.994 149 793.70 1.986 163 788.09 1.972 63 786.38 1.968 72 783.69 1.961 123 778.08 1.947 180 773.32 1.935 78 771.85 1.932 106 770.51 1.928 78 769.17 1.925 79 768.80 1.924 78 767.46 1.921 64 766.36 1.918 67 764.53 1.913 55 694.46 1.738 46 690.67 1.729 60 689.33 1.725 65 687.87 1.722 55 653.44 1.636 214 644.04 1.612 201 536.50 1.343 1000 517.46 1.295 843 377.20 0.944 850
in CDCl3
liquid film
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