ALPHA-PINENE OXIDE

Mass

MS-NW-7595          
2,3-epoxypinane
C10H16O             (Mass of molecular ion:    152)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.3
      17.0       1.2
      18.0       5.1
      27.0      15.7
      28.0       1.9
      29.0       8.5
      38.0       1.7
      39.0      27.2
      40.0       5.2
      41.0      51.7
      42.0       4.0
      43.0      14.5
      50.0       2.9
      51.0       9.2
      52.0       4.0
      53.0      17.3
      54.0       5.7
      55.0      45.1
      56.0       4.9
      57.0       1.6
      58.0       1.2
      62.0       1.3
      63.0       3.9
      64.0       1.6
      65.0      10.9
      66.0      14.7
      67.0      48.1
      68.0       8.7
      69.0      33.2
      70.0       4.4
      71.0       1.0
      77.0      21.1
      78.0       6.5
      79.0      18.7
      80.0       4.5
      81.0      27.8
      82.0      13.3
      83.0      39.0
      84.0       4.6
      89.0       1.3
      91.0      43.4
      92.0      16.6
      93.0      68.4
      94.0      10.2
      95.0      43.8
      96.0       7.2
      97.0       6.4
      98.0       1.2
     103.0       3.2
     104.0       1.9
     105.0       9.6
     106.0       4.3
     107.0       8.9
     108.0     100.0
     109.0      37.8
     110.0       8.6
     111.0       3.8
     115.0       4.3
     116.0       1.4
     117.0       8.6
     118.0       1.4
     119.0      39.6
     120.0       4.2
     121.0       2.4
     123.0       2.4
     131.0       1.3
     132.0       5.5
     133.0       1.9
     134.0      14.5
     135.0       2.7
     136.0       1.0
     137.0      12.5
     138.0       1.4
     152.0       7.9

Assign. Shift(ppm) A 3.066 B 2.00 C 1.98 D 1.947 E 1.911 F 1.73 G 1.623 J *1 1.342 K *1 1.294 L *1 0.944

     Hz     ppm     Int.

   1228.15   3.074    108
   1226.93   3.071    113
   1224.00   3.063    111
   1222.78   3.060    112
    811.77   2.032     70
    808.59   2.024     80
    803.83   2.012     64
    802.00   2.007     70
    800.54   2.004     46
    798.58   1.999     56
    796.51   1.994    149
    793.70   1.986    163
    788.09   1.972     63
    786.38   1.968     72
    783.69   1.961    123
    778.08   1.947    180
    773.32   1.935     78
    771.85   1.932    106
    770.51   1.928     78
    769.17   1.925     79
    768.80   1.924     78
    767.46   1.921     64
    766.36   1.918     67
    764.53   1.913     55
    694.46   1.738     46
    690.67   1.729     60
    689.33   1.725     65
    687.87   1.722     55
    653.44   1.636    214
    644.04   1.612    201
    536.50   1.343   1000
    517.46   1.295    843
    377.20   0.944    850