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TRIPHENYLGERMANIUM CHLORIDE

Product Name TRIPHENYLGERMANIUM CHLORIDE

CAS1626-24-0

MFC18H15ClGe

MW339.4

¹³CNMR

Mass

MS-NW-8005          
chlorotriphenylgermane
C18H15ClGe          (Mass of molecular ion:    340)

   Source Temperature: 160 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      18.0       2.2
      27.0       1.0
      50.0       2.5
      51.0      14.9
      52.0       1.1
      77.0      22.4
      78.0       2.1
      95.0       1.0
      97.0       1.3
      99.0       1.8
     105.0       5.6
     107.0       9.1
     108.0       2.1
     109.0      11.8
     111.0       5.2
     121.0       1.0
     123.0       1.3
     125.0       1.4
     147.0       7.5
     149.0       9.7
     150.0       3.8
     151.0      12.5
     152.0       4.9
     153.0       3.5
     154.0     100.0
     155.0      13.1
     223.0       1.2
     224.0       1.3
     225.0       1.8
     226.0       2.1
     227.0       2.0
     228.0       1.0
     259.0      19.6
     260.0       2.8
     261.0      31.8
     262.0      11.5
     263.0      43.3
     264.0       8.0
     265.0      18.6
     266.0       2.5
     267.0       2.5
     301.0       1.6
     303.0       2.0
     304.0       1.0
     305.0       2.4
     336.0       6.4
     337.0       1.4
     338.0      10.4
     339.0       4.6
     340.0      14.0
     341.0       3.6
     342.0       6.4
     343.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₈ H₁₅ Cl Ge	0.030 g : 0.5 ml CDCl₃
chlorotriphenylgermane

    Assign.     Shift(ppm)

      A             7.637
      B             7.46
      C             7.43

     Hz     ppm     Int.

   3058.72   7.654     95
   3056.64   7.649    627
   3055.05   7.645    807
   3053.83   7.642    403
   3051.03   7.635    297
   3049.07   7.630    771
   3047.12   7.625    834
   2995.61   7.496     49
   2994.02   7.492    102
   2992.43   7.488     79
   2991.09   7.485     67
   2986.94   7.474    311
   2986.21   7.473    336
   2983.52   7.466    195
   2981.69   7.461    420
   2979.98   7.457    808
   2978.03   7.452   1000
   2976.44   7.448    481
   2973.27   7.440    315
   2972.17   7.437    474
   2970.83   7.434    715
   2969.24   7.430    247
   2965.94   7.422    150
   2964.60   7.418    264
   2963.62   7.416    145
   2962.04   7.412    180

in CDCl3

KBr disc

nujol mull

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