TETRA-N-BUTYLGERMANE

Mass

MS-NW-8639          
tetrabutylgermane
C16H36Ge            (Mass of molecular ion:    302)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      27.0       2.6
      28.0       1.3
      29.0       8.6
      39.0       1.4
      41.0       5.7
      55.0      30.4
      56.0       1.8
      57.0       2.4
      70.0       2.3
      71.0       1.5
      72.0       3.0
      73.0       4.5
      74.0       4.6
      75.0       4.8
      76.0       1.4
      77.0       3.4
      85.0       5.3
      87.0      14.2
      88.0       2.7
      89.0      18.7
      90.0       3.4
      91.0      14.5
      93.0       2.7
      99.0       5.3
     100.0       1.4
     101.0      11.2
     102.0       3.1
     103.0      13.1
     104.0       2.8
     105.0       9.1
     107.0       1.6
     127.0       2.6
     128.0       3.0
     129.0      42.6
     130.0       6.2
     131.0      55.8
     132.0      20.2
     133.0      69.5
     134.0       3.8
     135.0      14.4
     185.0      56.3
     186.0       5.6
     187.0      74.6
     188.0      28.0
     189.0     100.0
     190.0       8.9
     191.0      20.8
     192.0       1.8
     241.0      18.8
     242.0       2.5
     243.0      24.8
     244.0      10.3
     245.0      33.4
     246.0       4.4
     247.0       7.1

Assign. Shift(ppm) A 1.316 B 0.888 C 0.693

     Hz     ppm     Int.

    545.78   1.366     45
    541.87   1.356     75
    539.43   1.350     82
    535.16   1.340    275
    534.06   1.337    231
    530.88   1.329    381
    527.59   1.321    609
    523.32   1.310    516
    519.78   1.301    515
    516.36   1.293    234
    513.55   1.285    125
    506.96   1.269     44
    371.58   0.930     34
    364.75   0.913    108
    361.94   0.906    460
    359.01   0.899    248
    356.45   0.892    354
    354.86   0.888   1000
    350.95   0.879    256
    349.37   0.875    254
    347.66   0.870    406
    340.70   0.853     30
    291.99   0.731     37
    290.16   0.727     42
    284.91   0.713    294
    282.23   0.707    170
    280.52   0.702    224
    276.73   0.693    341
    273.19   0.684    226
    268.55   0.672    276