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MassMS-NW-9252 (1S-(1alpha,2beta,4beta))-2-chloro-1-isopropyl-4-methylcyclohexane C10H19Cl (Mass of molecular ion: 174)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 6.5 29.0 5.4 36.0 1.1 39.0 7.9 40.0 1.3 41.0 22.3 42.0 4.4 43.0 16.4 51.0 1.5 53.0 7.5 54.0 8.1 55.0 32.5 56.0 11.0 57.0 10.0 65.0 2.0 66.0 1.0 67.0 28.3 68.0 9.6 69.0 17.8 70.0 4.7 75.0 2.1 77.0 3.5 79.0 4.9 80.0 11.1 81.0 100.0 82.0 34.5 83.0 14.6 84.0 1.5 89.0 3.1 91.0 2.3 93.0 2.3 94.0 8.6 95.0 83.7 96.0 23.0 97.0 5.9 109.0 10.1 110.0 2.6 123.0 47.8 124.0 4.9 137.0 1.2 138.0 41.3 139.0 4.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H19 Cl 0.05 ml : 0.5 ml CDCl3 (1S-(1alpha,2beta,4beta))-2-chloro-1-isopropyl-4-methylcyclohexane 
Assign. Shift(ppm)
A 3.775 B 2.353 C 2.228 D 1.713 E 1.44 F 1.381 G 0.99 J 0.92 K *1 0.918 L *1 0.917 M 0.772
Hz ppm Int.1521.97 3.809 67 1517.70 3.798 51 1510.74 3.781 129 1506.59 3.770 96 1499.76 3.753 74 1495.61 3.743 52 948.97 2.375 55 946.04 2.368 58 942.02 2.358 73 939.09 2.350 77 934.94 2.340 58 932.13 2.333 59 897.95 2.247 63 896.12 2.243 71 894.04 2.238 64 891.72 2.232 48 888.67 2.224 50 886.72 2.219 61 884.52 2.214 59 882.45 2.209 59 694.46 1.738 83 691.89 1.732 113 690.19 1.727 125 689.33 1.725 131 682.01 1.707 106 680.91 1.704 116 679.44 1.701 134 677.61 1.696 136 675.17 1.690 72 581.05 1.454 42 577.76 1.446 45 575.32 1.440 45 574.58 1.438 45 572.88 1.434 52 571.29 1.430 55 569.34 1.425 101 566.77 1.419 87 564.21 1.412 80 561.28 1.405 89 557.74 1.396 196 552.49 1.383 62 549.44 1.375 94 546.39 1.368 187 538.33 1.348 63 534.42 1.338 74 420.41 1.052 58 416.63 1.043 74 406.49 1.018 79 404.54 1.013 68 402.83 1.008 50 394.29 0.987 67 389.89 0.976 45 385.50 0.965 75 383.18 0.959 54 381.47 0.955 54 378.42 0.947 78 375.98 0.941 133 374.39 0.937 147 370.97 0.929 828 369.38 0.925 850 363.77 0.911 986 363.28 0.909 1000 351.93 0.881 63 312.01 0.781 789 305.05 0.764 793
in CDCl3
liquid film
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