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(-)-MENTHYL CHLORIDE

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(-)-MENTHYL CHLORIDE Basic information
(-)-MENTHYL CHLORIDE Chemical Properties
  • Melting point:−20-−16.5 °C(lit.)
  • Boiling point:101-101.5 °C21 mm Hg(lit.)
  • Density 0.936 g/mL at 25 °C(lit.)
  • refractive index n20/D 1.464
  • Flash point:174 °F
  • optical activity[α]20/D 52.4°, neat
  • BRN 1902297
Safety Information
  • Safety Statements 23-24/25
  • WGK Germany 3
  • HazardClass IRRITANT
MSDS
(-)-MENTHYL CHLORIDE Usage And Synthesis
  • Uses2-Chloro-4-methyl-1-(1-methylethyl)-Cyclohexane is a useful building block for organic synthesis.
  • Purification MethodsDissolve menthyl chloride in pet ether (b 40-60o), wash with H2O, conc H2SO4 until no discoloration of the organic layer occurs (care with conc H2SO4 during shaking in a separating funnel), again with H2O and dry it (MgSO4). Evaporate and distil the residual oil through a Claisen head with a Vigreux neck ( p 11) of ca 40 cm length. [Smith & Wright J Org Chem 17 1116 1952, Barton et al. J Chem Soc 453 1952, Beilstein 5 III 134.]
(-)-MENTHYL CHLORIDE Preparation Products And Raw materials
(-)-MENTHYL CHLORIDE(16052-42-9)Related Product Information
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