2-Amino-5-methylpyridine

Mass

MS-NW-3572          
2-amino-5-methylpyridine
C6H8N2              (Mass of molecular ion:    108)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       1.4
      27.0       6.4
      28.0       8.8
      30.0       2.0
      37.0       1.2
      38.0       2.5
      39.0       7.6
      40.0       2.1
      41.0       5.7
      42.0       1.4
      43.0       1.7
      50.0       3.0
      51.0       5.2
      52.0       7.1
      53.0      16.9
      54.0       6.0
      55.0       2.1
      56.0       2.1
      63.0       1.3
      64.0       1.3
      65.0       2.2
      66.0       2.0
      67.0       1.3
      68.0       2.4
      78.0       1.8
      79.0       1.6
      80.0      49.0
      81.0      19.8
      82.0       1.5
      91.0       2.0
      92.0       1.3
     107.0      41.5
     108.0     100.0
     109.0       7.7

Parameter ppm Hz D(A) 7.79 D(B) 7.12 D(C) 6.32 D(D) 2.12 J(A,B) 2.4 J(A,C) 0.8 J(A,D) 0.8 J(B,C) 8.4 J(B,D) 0.6 J(C,D) 0.2 D(E) 4.67 BELL,C.L. ET AL. J.HETEROCYCL.CHEM. 2, 420 (1965) J(C,D):LESS THAN 0.2HZ.

     Hz     ppm     Int.

   2338.95   7.796     91
   2338.21   7.794    127
   2337.48   7.792    118
   2336.59   7.789    120
   2335.85   7.786    130
   2335.11   7.784     93
   2141.78   7.139     67
   2141.20   7.137     69
   2139.36   7.131     69
   2138.89   7.130     68
   2133.32   7.111     74
   2132.84   7.109     76
   2130.95   7.103     74
   2130.48   7.102     72
   1900.41   6.335    140
   1899.88   6.333    140
   1892.00   6.307    132
   1891.48   6.305    129
   1401.02   4.670   1000
    635.97   2.120    850