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MassMS-NW-8460 p-phenetidine C8H11NO (Mass of molecular ion: 137)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
26.0 1.6 27.0 8.1 28.0 6.4 29.0 3.9 38.0 1.2 39.0 6.3 41.0 2.4 42.0 1.0 50.0 1.0 51.0 2.5 52.0 8.8 53.0 16.4 54.0 5.1 55.0 1.3 61.0 1.1 63.0 2.7 64.0 2.1 65.0 8.4 66.0 1.7 78.0 1.0 79.0 1.7 80.0 42.8 81.0 9.8 82.0 1.8 91.0 1.3 92.0 3.0 108.0 100.0 109.0 66.2 110.0 4.6 137.0 61.1 138.0 5.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N O 0.04 ml : 0.5 ml CDCl3 p-phenetidine 
Assign. Shift(ppm)
A 6.69 B 6.63 C 3.929 D 3.33 E 1.348 J(C,E)=7.0HZ
Hz ppm Int.608.19 6.791 100 607.50 6.784 89 605.25 6.759 73 601.94 6.722 101 599.06 6.689 632 596.88 6.665 164 596.25 6.658 167 594.06 6.634 655 591.25 6.602 119 587.94 6.565 79 585.69 6.540 101 585.06 6.533 103 362.75 4.051 122 355.75 3.973 436 348.75 3.895 460 341.88 3.818 152 298.19 3.330 326 127.75 1.427 501 126.06 1.408 35 120.81 1.349 1000 113.81 1.271 438
in CDCl3
CCl4 solution
liquid film
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