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MS-NW-2387 (p-hydroxyphenyl)acetic acid C8H8O3 (Mass of molecular ion: 152)
Source Temperature: 190 °C Sample Temperature: 130 °C Direct, 75 eV
27.0 2.5 39.0 3.5 45.0 1.3 50.0 2.2 51.0 4.9 52.0 2.5 53.0 3.0 55.0 1.5 63.0 1.4 77.0 13.5 78.0 3.8 79.0 2.3 107.0 100.0 108.0 8.2 109.0 1.1 152.0 28.7 153.0 2.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C8 H8 O3 0.041 g : 0.5 ml DMSO-d6 (p-hydroxyphenyl)acetic acid Assign. Shift(ppm)
A 12. B 9.3 C 7.044 D 6.702 E 3.420
Hz ppm Int.
2822.23 7.062 58 2819.30 7.055 480 2817.47 7.050 199 2812.89 7.039 179 2810.69 7.033 548 2685.40 6.720 76 2682.66 6.713 640 2680.64 6.708 231 2676.06 6.697 189 2674.05 6.691 588 2671.12 6.684 69 1367.15 3.421 1000
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