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15374-45-5

1,2-BIS(1-NAPHTHYL)ETHANE

Product Name 1,2-BIS(1-NAPHTHYL)ETHANE

CAS15374-45-5

MFC22H18

MW282.38

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  • 15374-45-5_ms
    Mass 

    MS-IW-3984          
1,1'-ethylenedinaphthalene
C22H18              (Mass of molecular ion:    282)


       Source Temperature: 160 °C
   Sample Temperature: 130 °C
   Direct, 75 eV


         115.0       8.9
     139.0       2.5
     141.0     100.0
     142.0      12.4
     153.0       1.0
     282.0      25.7
     283.0       6.2

400 MHz in CDCl3

  • 15374-45-5_1hnmr

    1H NMR 399.65 MHz
    C22 H18 0.045 g : 0.5 ml CDCl3
    1,1'-ethylenedinaphthalene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.105
      B             7.864
      C             7.727
      D             7.51
      E             7.48
      F             7.378
      G             7.327
      J             3.496
     
     ASSIGNED BY C-H COSY.
  

         Hz     ppm     Int.


       3244.26   8.118    128
   3243.16   8.116    149
   3234.74   8.094    156
   3147.71   7.877    143
   3145.63   7.871    106
   3140.14   7.858    178
   3138.31   7.853    157
   3092.29   7.738    165
   3084.23   7.718    185
   3009.52   7.531     60
   3007.93   7.527     78
   3002.81   7.514    161
   3001.22   7.510    152
   2999.76   7.506     77
   2995.00   7.495    315
   2992.92   7.489    301
   2988.04   7.477     82
   2987.06   7.475    146
   2985.60   7.471    160
   2980.22   7.458     68
   2978.88   7.454     59
   2957.15   7.400    139
   2950.07   7.382    248
   2942.02   7.362    230
   2930.91   7.334    216
   2929.81   7.331    235
   2923.95   7.317    124
   2922.85   7.314    121
   1397.22   3.497   1000

in CDCl3

  • 15374-45-5_13cnmr

KBr disc

  • 15374-45-5_ir1_2

nujol mull

  • 15374-45-5_ir2

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