Diphenylphosphinic Chloride
Product Name Diphenylphosphinic Chloride
CAS1499-21-4
MFC12H10ClOP
MW236.63
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MS-IW-8116 diphenylphosphinic chloride C12H10ClOP (Mass of molecular ion: 236)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 1.0 47.0 3.0 50.0 3.5 51.0 13.9 74.0 1.3 75.0 1.4 76.0 2.9 77.0 25.1 78.0 2.2 95.0 1.3 99.5 2.8 100.0 1.8 107.0 3.2 123.0 1.0 128.0 1.0 143.0 14.7 144.0 1.0 145.0 4.9 151.0 1.7 152.0 8.6 153.0 4.1 154.0 3.1 159.0 1.8 170.0 1.1 171.0 1.6 173.0 2.0 183.0 4.0 199.0 40.8 200.0 9.9 201.0 46.4 202.0 6.1 219.0 1.6 235.0 100.0 236.0 50.1 237.0 39.4 238.0 16.6 239.0 2.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H10 Cl O P 0.05 ml : 0.5 ml CDCl3 diphenylphosphinic chloride Assign. Shift(ppm)
A 7.867 B 7.567 C 7.491
Hz ppm Int.
3157.96 7.902 140 3156.25 7.898 608 3154.91 7.895 820 3153.44 7.891 426 3150.02 7.882 267 3147.95 7.877 1000 3146.48 7.874 836 3143.68 7.867 155 3141.85 7.862 630 3140.50 7.859 852 3139.16 7.855 424 3135.62 7.846 261 3133.54 7.841 998 3132.08 7.838 841 3035.40 7.596 116 3034.18 7.593 219 3033.57 7.591 179 3032.23 7.588 253 3030.88 7.584 165 3029.05 7.580 170 3026.98 7.575 516 3024.54 7.568 555 3022.58 7.564 224 3020.63 7.559 301 3019.29 7.555 512 3018.68 7.554 407 3017.33 7.550 535 3015.99 7.547 277 3012.08 7.537 45 3010.99 7.535 43 3005.86 7.522 80 3004.27 7.518 195 3003.17 7.515 487 3002.44 7.513 665 3001.10 7.510 380 3000.00 7.507 258 2998.90 7.504 518 2998.17 7.502 686 2996.22 7.498 638 2994.75 7.494 960 2993.16 7.490 381 2991.82 7.487 559 2990.48 7.483 956 2989.14 7.480 469 2987.67 7.476 523 2986.45 7.473 349 2984.86 7.469 234 2983.28 7.465 450 2982.30 7.463 314
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