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2-Piperidineethanol

Product Name 2-Piperidineethanol

CAS1484-84-0

MFC7H15NO

MW129.2

¹³CNMR

Mass

MS-NW-9203          
2-piperidineethanol
C7H15NO             (Mass of molecular ion:    129)

   Source Temperature: 250 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       4.8
      27.0       3.1
      28.0       7.3
      29.0       3.0
      30.0       9.3
      31.0       2.4
      39.0       2.8
      41.0       6.1
      42.0       6.9
      43.0       4.5
      44.0       4.5
      45.0       1.1
      53.0       1.2
      54.0       2.8
      55.0       6.8
      56.0      14.8
      57.0       2.6
      67.0       1.7
      68.0       1.7
      69.0       1.0
      70.0       2.8
      72.0       4.0
      82.0       2.5
      83.0       1.2
      84.0     100.0
      85.0       6.2
      86.0       1.0
      98.0       4.6
     100.0       1.0
     110.0       1.3
     111.0       1.0
     128.0       1.6
     129.0       1.4

90 MHz in CDCl3

400 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₁₅ N O	0.040 g : 0.5 ml CDCl₃
2-piperidineethanol

    Assign.     Shift(ppm)

      A     *1      3.77
      B     *1      3.75
      C             3.32
      D             3.02
      E             2.74
      F             2.60
      G          1.84 to 1.19
      J             1.59

     Hz     ppm     Int.

    348.44   3.891     35
    343.06   3.831    418
    342.38   3.823    401
    341.13   3.809     88
    340.50   3.802     82
    337.00   3.763    895
    332.19   3.710    377
    330.69   3.693    408
    327.94   3.662     32
    325.44   3.634     34
    319.75   3.571     36
    297.63   3.324   1000
    282.69   3.157     30
    280.38   3.131     68
    279.06   3.116     83
    277.31   3.097     90
    275.00   3.071     55
    269.94   3.015     61
    267.13   2.983    165
    266.75   2.979    165
    264.50   2.954    180
    257.50   2.876     51
    255.31   2.851     39
    254.75   2.845     40
    251.44   2.808     95
    248.50   2.775     85
    248.19   2.772     85
    247.38   2.763     94
    245.19   2.738    179
    242.00   2.703    178
    239.50   2.675    119
    235.13   2.626    147
    234.00   2.613    170
    232.56   2.597    145
    229.56   2.564     62
    229.19   2.560     62
    226.38   2.528     34
    225.13   2.514     37
    221.56   2.474     71
    220.13   2.458     48
    218.56   2.441     57
    170.69   1.906     32
    169.44   1.892     49
    167.81   1.874     63
    166.56   1.860     82
    163.31   1.824    101
    161.69   1.806    136
    160.00   1.787    132
    157.81   1.763    123
    155.00   1.731     85
    153.06   1.710    139
    149.25   1.667    534
    147.13   1.643    218
    146.44   1.636    235
    143.75   1.606    784
    140.44   1.569    329
    137.94   1.541    870
    136.56   1.525    480
    134.56   1.503    334
    132.56   1.481    370
    131.44   1.468    331
    126.69   1.415    219
    125.75   1.405    195
    125.19   1.398    193
    124.19   1.387    174
    120.31   1.344    225
    118.63   1.325    238
    117.50   1.312    207
    116.06   1.296    172
    113.19   1.264    102
    111.00   1.240    128
    106.25   1.187     70
    102.81   1.148     31
    102.38   1.144     33
    101.94   1.139     34
    100.75   1.125     46
    100.31   1.121     43
    100.00   1.117     42
     96.75   1.081     57

¹H NMR	399.65 MHz
C₇ H₁₅ N O	0.034 g : 0.5 ml CDCl₃
2-piperidineethanol

    Assign.     Shift(ppm)

      A     *1      3.80
      B     *1      3.75
      C             3.2
      D             3.032
      E             2.740
      F             2.597
      G             1.810
      J             1.61
      K             1.57
      L     *2      1.42
      M     *2      1.35
      N             1.35
     
     ASSIGNED BY H-H COSY.
     90MHZ : HSP-03-798

     Hz     ppm     Int.

   1532.35   3.835    170
   1527.22   3.822    299
   1521.48   3.808    478
   1516.36   3.795    791
   1511.35   3.782    428
   1509.03   3.776    454
   1503.91   3.764    276
   1503.05   3.761    331
   1502.44   3.760    425
   1502.08   3.759    418
   1498.17   3.749    216
   1496.70   3.746    465
   1493.16   3.737    115
   1492.43   3.735    130
   1491.09   3.731    178
   1485.84   3.718    193
   1222.17   3.059    137
   1220.09   3.053    196
   1218.14   3.049    233
   1215.94   3.043    205
   1213.87   3.038    137
   1209.47   3.027    154
   1207.40   3.022    202
   1205.44   3.017    279
   1203.86   3.013    241
   1201.42   3.007    134
   1107.79   2.772    109
   1105.10   2.766    121
   1100.59   2.754    168
   1098.39   2.749    146
   1096.68   2.745    178
   1094.12   2.738    179
   1093.26   2.736    172
   1089.72   2.727    173
   1087.40   2.721    136
   1084.84   2.715    131
   1082.15   2.708    122
   1051.15   2.631    252
   1048.34   2.624    235
   1038.82   2.600    370
   1036.50   2.594    276
   1035.77   2.592    285
   1026.61   2.569    243
   1023.93   2.563    178
    732.30   1.833    118
    730.35   1.828    151
    728.76   1.824    166
    727.17   1.820    134
    725.22   1.815    130
    723.88   1.812    105
    721.19   1.805    139
    719.12   1.800    145
    717.77   1.796    195
    715.94   1.792    206
    713.01   1.785    132
    655.52   1.641    210
    652.83   1.634    210
    650.63   1.628    122
    649.05   1.625    124
    645.51   1.616    285
    642.70   1.609    439
    641.48   1.606    399
    640.87   1.604    409
    639.89   1.602    409
    636.96   1.594    689
    631.59   1.581   1000
    630.49   1.578    945
    625.61   1.566    955
    623.17   1.560    369
    621.09   1.555    291
    618.29   1.548    255
    582.15   1.457    181
    578.61   1.448    279
    574.95   1.439    133
    569.46   1.425    206
    565.92   1.417    331
    562.74   1.409    184
    556.88   1.394    136
    555.42   1.390    129
    554.81   1.389    126
    552.98   1.384    246
    550.42   1.378    152
    548.46   1.373    123
    543.33   1.360    173
    539.79   1.351    273
    535.89   1.341    154
    531.37   1.330    124
    527.47   1.320    216
    523.80   1.311    125
    498.29   1.247    125
    494.63   1.238    150
    487.43   1.220    151
    485.72   1.216    204
    483.76   1.211    189
    481.93   1.206    203
    474.61   1.188    172
    473.27   1.185    137
    470.83   1.179    187

in CDCl3

KBr disc

nujol mull

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