PHENYL-BETA-D-GLUCOPYRANOSIDE

Mass

MS-NW-2020          
phenyl beta-D-glucopyranoside
C12H16O6            (Mass of molecular ion:    256)

   Source Temperature: 200 °C
   Sample Temperature: 200 °C
   Direct, 75 eV

      15.0       2.9
      17.0       1.5
      18.0       8.4
      19.0       2.5
      26.0       1.4
      27.0       4.4
      28.0       3.7
      29.0       8.0
      30.0       2.5
      31.0       7.0
      38.0       1.7
      39.0       7.6
      40.0       3.7
      41.0       2.9
      42.0       2.9
      43.0       8.6
      44.0       2.5
      45.0       5.3
      47.0       1.4
      50.0       1.6
      51.0       3.2
      53.0       1.1
      55.0       6.0
      56.0       2.1
      57.0       8.8
      60.0       8.7
      61.0       5.4
      63.0       1.2
      65.0       5.9
      66.0       8.2
      68.0       1.1
      69.0       4.7
      70.0       1.6
      71.0       3.4
      72.0       1.3
      73.0       9.3
      74.0       1.4
      77.0       4.8
      85.0       7.3
      87.0       4.3
      89.0       1.2
      91.0       2.0
      94.0     100.0
      95.0       8.4
      96.0       1.3
      97.0       2.9
      98.0       1.5
      99.0       1.0
     107.0       1.2
     127.0       1.7
     145.0       1.5
     162.0       1.3

Assign. Shift(ppm) A 7.392 B 7.14 C 5.080 D *1 3.913 E *1 3.769 F 3.62 G 3.58 J 3.52

     Hz     ppm     Int.

   2963.13   7.415    421
   2955.32   7.395    706
   2947.02   7.375    595
   2859.50   7.156   1000
   2853.27   7.140    741
   2851.07   7.134    696
   2850.22   7.132    703
   2847.05   7.124    225
   2846.07   7.122    241
   2034.06   5.090    528
   2030.27   5.081     51
   2026.61   5.071    551
   1572.14   3.934    234
   1570.07   3.929    266
   1559.69   3.903    364
   1557.62   3.898    348
   1517.33   3.797     35
   1514.28   3.790    291
   1511.72   3.783     73
   1509.16   3.777    342
   1505.37   3.767     38
   1504.88   3.766     38
   1501.95   3.759    212
   1496.70   3.746    244
   1458.01   3.649    142
   1448.85   3.626    446
   1445.80   3.618     57
   1440.31   3.604    889
   1436.77   3.596    187
   1432.37   3.585    677
   1430.30   3.579    367
   1427.00   3.571    263
   1424.80   3.566    244
   1423.34   3.562    241
   1420.41   3.555     44
   1419.80   3.553     41
   1419.31   3.552     41
   1419.07   3.551     41
   1415.16   3.541    418
   1410.77   3.531     38
   1406.37   3.520    304
   1396.85   3.496    139