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Trichloropropylsilane

Product Name Trichloropropylsilane

CAS141-57-1

MFC3H7Cl3Si

MW177.53

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¹HNMR

¹³CNMR

IR1

Mass

MS-NW-3279          
trichloro(propyl)silane
C3H7Cl3Si           (Mass of molecular ion:    176)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       1.4
      26.0       1.9
      27.0      14.9
      28.0       3.4
      29.0      12.2
      38.0       1.7
      39.0      13.4
      40.0       2.6
      41.0      22.7
      42.0      32.6
      43.0      61.1
      44.0       2.1
      49.0       1.9
      53.0       1.0
      63.0      18.5
      64.0       1.5
      65.0       6.8
      98.0       7.7
      99.0       5.9
     100.0       5.6
     101.0       4.2
     102.0       1.2
     112.0      11.7
     113.0       3.3
     114.0       8.0
     115.0       2.2
     116.0       1.7
     125.0      15.0
     126.0       2.0
     127.0      10.0
     128.0       1.1
     129.0       1.9
     133.0      64.2
     134.0       3.4
     135.0      63.5
     136.0       3.5
     137.0      21.8
     138.0       1.3
     139.0       3.7
     140.0     100.0
     141.0      11.0
     142.0      67.5
     143.0       6.7
     144.0      12.6
     145.0       1.3
     161.0      22.0
     162.0       1.9
     163.0      21.7
     164.0       1.8
     165.0       7.5
     167.0       1.0
     175.0       1.2
     176.0       3.8
     177.0       1.5
     178.0       3.9
     180.0       1.4

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₃ H₇ Cl₃ Si	0.05 ml : 0.5 ml CDCl₃
trichloro(propyl)silane

    Assign.     Shift(ppm)

      A             1.641
      B             1.403
      C             1.072

     Hz     ppm     Int.

    676.15   1.692     33
    675.17   1.690     34
    670.78   1.679     30
    668.58   1.673    113
    667.97   1.672    104
    665.16   1.665     44
    663.57   1.661     65
    660.89   1.654    183
    657.71   1.646     80
    656.25   1.643     89
    654.66   1.639     93
    653.44   1.636    157
    652.22   1.632    179
    650.39   1.628     78
    648.93   1.624     66
    647.46   1.621     43
    645.02   1.614    142
    643.19   1.610     39
    638.06   1.597     45
    637.21   1.595     44
    571.78   1.431     30
    567.63   1.421    370
    563.35   1.410    117
    561.89   1.406    206
    559.45   1.400    264
    558.84   1.399    264
    557.62   1.396    164
    556.15   1.392    127
    551.64   1.381    230
    551.03   1.379    237
    435.06   1.089    614
    427.86   1.071   1000
    423.34   1.060     35
    420.41   1.052    520

¹H NMR	89.56 MHz
C₃ H₇ Cl₃ Si	0.04 ml : 0.5 ml CDCl₃
trichloro(propyl)silane

    Assign.     Shift(ppm)

      A             1.61
      B             1.41
      C             1.07

     Hz     ppm     Int.

    162.38   1.814     32
    161.69   1.806     41
    158.63   1.772     62
    156.19   1.744     38
    155.25   1.734     67
    154.69   1.728     79
    153.25   1.712     63
    152.75   1.706     51
    151.50   1.692    139
    149.38   1.668    123
    147.81   1.651     76
    146.19   1.633    126
    145.75   1.628    104
    145.00   1.620    151
    144.06   1.609    196
    142.00   1.586    126
    140.56   1.570     86
    140.00   1.564    112
    138.94   1.552    186
    137.25   1.533    200
    135.44   1.513     75
    133.81   1.495    137
    132.88   1.484    237
    131.88   1.473    312
    131.25   1.466    275
    130.50   1.458    272
    129.44   1.446    149
    128.25   1.433    122
    127.38   1.423    189
    125.88   1.406     74
    125.06   1.397    173
    123.31   1.377    123
    122.81   1.372    132
    122.44   1.368    140
    121.50   1.357    108
    119.75   1.338     47
    117.75   1.315    148
    115.44   1.289     88
    115.06   1.285     86
    103.19   1.153    172
    102.44   1.144    330
    101.75   1.137    403
    100.88   1.127    175
    100.25   1.120    124
     95.75   1.070   1000
     92.88   1.038     85
     89.13   0.996    181
     88.44   0.988    280
     86.63   0.968     69

in CDCl3

liquid film

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