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13548-69-1More Spectrum > 2,7-Diaminofluorene dihydrochloride(13548-69-1)MS
2,7-Diaminofluorene dihydrochloride
Product Name 2,7-Diaminofluorene dihydrochloride
CAS13548-69-1
MFC13H14Cl2N2
MW269.17
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MassMS-NW-2332 2,7-fluorenediamine dihydrochloride C13H12N2 2HCl (Mass of molecular ion: 196)
Source Temperature: 200 °C Sample Temperature: 140 °C Direct, 75 eV
18.0 2.7 28.0 1.0 35.0 2.4 36.0 22.5 38.0 7.4 63.0 1.0 70.5 1.0 83.5 6.0 84.0 1.9 97.5 7.0 98.0 8.5 98.5 1.1 115.0 1.0 139.0 2.3 140.0 1.4 141.0 1.0 151.0 2.4 152.0 2.6 153.0 1.0 166.0 1.3 167.0 5.9 168.0 4.4 178.0 2.2 179.0 2.5 180.0 11.7 181.0 2.1 193.0 1.1 194.0 1.3 195.0 35.7 196.0 100.0 197.0 14.8 198.0 1.1
400 MHz in D2O
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1H NMR 399.65 MHz C13 H12 N2 0.042 g : 0.5 ml D2O 2,7-fluorenediamine dihydrochloride 
Assign. Shift(ppm)
A 7.339 B 7.294 C 7.263 D 3.134 SOLVENT SIGNAL REMOVED
Hz ppm Int.2933.72 7.341 674 2932.62 7.338 704 2926.88 7.324 26 2920.90 7.309 351 2912.96 7.289 1000 2905.88 7.272 631 2903.93 7.267 559 2897.71 7.251 224 2895.75 7.246 211 1252.44 3.134 589
KBr disc
nujol mull
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