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13548-69-1

2,7-Diaminofluorene dihydrochloride

Product Name 2,7-Diaminofluorene dihydrochloride

CAS13548-69-1

MFC13H14Cl2N2

MW269.17

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  • 13548-69-1_ms
    Mass

    MS-NW-2332          
    2,7-fluorenediamine dihydrochloride
    C13H12N2 2HCl       (Mass of molecular ion:    196)
    

       Source Temperature: 200 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          18.0       2.7
          28.0       1.0
          35.0       2.4
          36.0      22.5
          38.0       7.4
          63.0       1.0
          70.5       1.0
          83.5       6.0
          84.0       1.9
          97.5       7.0
          98.0       8.5
          98.5       1.1
         115.0       1.0
         139.0       2.3
         140.0       1.4
         141.0       1.0
         151.0       2.4
         152.0       2.6
         153.0       1.0
         166.0       1.3
         167.0       5.9
         168.0       4.4
         178.0       2.2
         179.0       2.5
         180.0      11.7
         181.0       2.1
         193.0       1.1
         194.0       1.3
         195.0      35.7
         196.0     100.0
         197.0      14.8
         198.0       1.1
    

400 MHz in D2O

  • 13548-69-1_1hnmr

    1H NMR 399.65 MHz
    C13 H12 N2 0.042 g : 0.5 ml D2O
    2,7-fluorenediamine dihydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.339 B 7.294 C 7.263 D 3.134 SOLVENT SIGNAL REMOVED

         Hz     ppm     Int.
    

       2933.72   7.341    674
       2932.62   7.338    704
       2926.88   7.324     26
       2920.90   7.309    351
       2912.96   7.289   1000
       2905.88   7.272    631
       2903.93   7.267    559
       2897.71   7.251    224
       2895.75   7.246    211
       1252.44   3.134    589
    

KBr disc

  • 13548-69-1_ir1_2

nujol mull

  • 13548-69-1_ir2