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MS-NW-4054 o-diethylbenzene C10H14 (Mass of molecular ion: 134)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.0 27.0 6.0 29.0 2.7 38.0 1.0 39.0 8.7 41.0 7.6 50.0 3.1 51.0 7.8 52.0 2.3 53.0 2.7 57.5 2.3 58.0 1.6 58.5 1.1 62.0 1.5 63.0 4.9 64.0 1.5 65.0 6.6 74.0 1.4 75.0 1.3 76.0 1.1 77.0 14.9 78.0 5.9 79.0 10.2 89.0 2.5 91.0 28.7 92.0 2.7 93.0 4.0 102.0 1.9 103.0 10.1 104.0 7.4 105.0 97.3 106.0 9.3 115.0 8.2 116.0 2.5 117.0 14.8 118.0 2.7 119.0 100.0 120.0 10.0 133.0 1.3 134.0 50.6 135.0 5.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H14 0.04 ml : 0.5 ml CDCl3 o-diethylbenzene Assign. Shift(ppm)
A 7.14 B 2.64 C 1.217
Hz ppm Int.
641.31 7.161 32 639.13 7.137 1000 636.88 7.112 79 629.81 7.033 24 249.00 2.781 81 248.44 2.775 86 241.00 2.691 358 238.63 2.665 32 233.44 2.607 412 231.25 2.583 33 226.38 2.528 119 225.88 2.523 122 116.13 1.297 437 110.06 1.229 71 108.81 1.215 925 106.56 1.190 54 101.06 1.129 336
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