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MS-NW-8709 1-naphthylamine C10H9N (Mass of molecular ion: 143)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 2.1 50.0 1.1 51.0 1.6 57.5 2.2 58.5 4.1 62.0 1.4 63.0 3.2 65.0 1.7 70.5 4.8 71.5 7.8 74.0 1.1 75.0 1.2 76.0 1.1 77.0 1.4 88.0 1.1 89.0 3.8 90.0 1.1 113.0 1.6 114.0 2.4 115.0 31.0 116.0 17.9 117.0 3.2 126.0 1.3 140.0 2.0 141.0 1.0 142.0 5.3 143.0 100.0 144.0 11.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H9 N 0.041 g : 0.5 ml CDCl3 1-naphthylamine Assign. Shift(ppm)
A 7.77 B 7.75 C *1 7.43 D *1 7.40 E 7.290 F 7.261 G 6.716 J 4.04
Hz ppm Int.
3115.72 7.797 34 3111.45 7.786 278 3109.01 7.780 316 3107.06 7.775 61 3105.47 7.771 173 3103.15 7.765 527 3102.05 7.762 584 3100.22 7.758 157 3099.24 7.755 138 3095.83 7.747 292 3094.12 7.743 236 3093.38 7.741 328 3089.48 7.731 37 3088.87 7.729 36 2976.81 7.449 93 2975.10 7.445 158 2969.97 7.432 437 2968.26 7.428 384 2966.55 7.423 490 2963.50 7.416 1000 2960.45 7.408 409 2958.62 7.404 386 2956.79 7.399 418 2951.78 7.386 149 2949.95 7.382 96 2921.02 7.309 108 2919.56 7.306 165 2919.19 7.305 154 2911.62 7.286 499 2910.89 7.284 438 2907.47 7.276 818 2904.66 7.269 30 2900.51 7.258 734 2899.29 7.255 259 2892.33 7.238 294 2688.35 6.727 475 2686.89 6.724 463 2681.52 6.710 464 2679.93 6.706 464 1615.48 4.043 112
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