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MS-NW-0762 (+-)-alpha-methylbenzyl alcohol C8H10O (Mass of molecular ion: 122)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.2 27.0 2.8 38.0 1.3 39.0 4.9 43.0 17.6 45.0 3.1 50.0 6.6 51.0 16.1 52.0 4.1 53.0 2.1 53.5 7.0 62.0 1.2 63.0 2.9 65.0 1.6 74.0 2.6 75.0 1.6 76.0 1.7 77.0 38.1 78.0 19.2 79.0 76.9 80.0 5.4 91.0 2.2 102.0 1.3 103.0 6.3 104.0 9.5 105.0 8.4 106.0 1.1 107.0 100.0 108.0 7.7 121.0 6.3 122.0 35.8 123.0 3.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H10 O 10.5 mol% in CDCl3 (+-)-alpha-methylbenzyl alcohol Assign. Shift(ppm)
A 1.41 B 2.73 C 4.77 D 7.19 to 7.36
Hz ppm Int.
657.94 7.347 49 657.50 7.342 48 656.19 7.327 36 654.31 7.306 158 653.94 7.302 153 651.75 7.278 1000 650.50 7.264 305 648.94 7.246 191 646.75 7.222 41 643.75 7.188 30 436.88 4.879 41 430.38 4.806 127 423.88 4.733 131 417.44 4.662 45 244.56 2.731 174 129.13 1.442 822 122.63 1.370 794
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