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Borane-methyl sulfide complex

Product Name Borane-methyl sulfide complex

CAS13292-87-0

MFC2H10BS

MW76.97

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  • Mass 

    MS-IW-3829          
borane-dimethyl sulfide complex
C2H6S H3B           (Mass of molecular ion:     76)


       Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          15.0       1.4
      24.0       1.4
      26.0       2.0
      27.0       8.2
      35.0      18.1
      44.0       4.0
      45.0      35.9
      46.0      30.3
      47.0      79.8
      48.0       3.1
      49.0       3.8
      57.0       2.7
      58.0       3.4
      59.0       3.5
      61.0      38.0
      62.0     100.0
      63.0       5.0
      64.0       4.9

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C2 H6 S 0.05 ml : 0.5 ml CDCl3
    borane-dimethyl sulfide complex
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             2.264
      B             1.50
     
     J(B-11,B)=104HZ
  

         Hz     ppm     Int.


        905.03   2.265   1000
    754.76   1.889     21
    754.39   1.888     21
    650.76   1.629     24
    650.27   1.628     24
    545.65   1.366     24
    545.29   1.365     24
    544.80   1.364     24
    544.43   1.363     24
    441.28   1.105     21
    440.67   1.103     21

in CDCl3



liquid film



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