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MS-NW-3755 ethyl myristate C16H32O2 (Mass of molecular ion: 256)
Source Temperature: 200 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.0 27.0 5.1 28.0 2.7 29.0 14.4 39.0 2.4 41.0 16.2 42.0 4.1 43.0 19.6 45.0 4.6 54.0 1.2 55.0 12.8 56.0 3.5 57.0 12.0 60.0 7.7 61.0 9.9 67.0 1.9 68.0 1.1 69.0 8.0 70.0 10.0 71.0 5.2 73.0 11.8 74.0 1.5 81.0 1.6 83.0 4.7 84.0 3.3 85.0 2.6 87.0 1.7 88.0 100.0 89.0 13.7 95.0 1.5 97.0 3.9 98.0 3.7 101.0 47.4 102.0 4.2 111.0 1.9 115.0 5.1 129.0 1.9 143.0 4.7 144.0 1.0 157.0 11.3 158.0 1.3 171.0 2.0 185.0 1.3 199.0 1.9 211.0 8.5 212.0 1.3 213.0 7.0 214.0 1.2 227.0 1.7 256.0 11.9 257.0 2.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C16 H32 O2 0.04 ml : 0.5 ml CDCl3 ethyl myristate Assign. Shift(ppm)
A 4.120 B 2.28 C 1.61 D 1.49 to 1.04 E 1.251 F 0.89 J(A,E)=7.1HZ.
Hz ppm Int.
379.94 4.243 31 372.75 4.163 109 365.63 4.083 114 358.56 4.004 37 204.94 2.289 50 197.13 2.202 43 124.19 1.387 24 119.06 1.330 185 112.69 1.259 1000 112.00 1.251 709 104.75 1.170 135 84.13 0.940 26 82.94 0.927 23 78.81 0.880 89
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