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MassMS-KW-0164 3-(chloromethyl)heptane C8H17Cl (Mass of molecular ion: 148)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 5.5 29.0 8.8 36.0 1.8 39.0 4.2 41.0 19.2 42.0 3.7 43.0 19.1 53.0 1.6 55.0 20.4 56.0 7.0 57.0 100.0 58.0 4.5 69.0 4.2 70.0 5.9 71.0 1.5 83.0 5.4 98.0 6.0 99.0 18.4 100.0 1.4 112.0 1.7 119.0 2.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H17 Cl 0.05 ml : 0.5 ml CDCl3 3-(chloromethyl)heptane 
Assign. Shift(ppm)
A *1 3.543 B *1 3.526 C 1.590 D 1.43 E 1.30 F 0.906 G 0.894
Hz ppm Int.1426.88 3.571 42 1422.00 3.559 51 1416.14 3.544 391 1414.18 3.539 393 1411.13 3.531 384 1409.06 3.526 381 1403.32 3.512 45 1398.19 3.499 42 636.23 1.592 90 630.00 1.577 82 588.75 1.474 65 582.15 1.457 112 581.18 1.455 156 574.71 1.439 252 573.73 1.436 189 568.48 1.423 178 567.26 1.420 270 564.82 1.414 68 561.16 1.405 179 560.06 1.402 131 557.13 1.395 93 553.59 1.386 134 550.66 1.378 72 547.12 1.369 112 544.19 1.362 96 540.65 1.353 80 538.33 1.348 153 535.89 1.341 86 532.35 1.333 122 530.27 1.327 153 528.08 1.322 133 524.90 1.314 225 520.75 1.304 247 516.97 1.294 203 514.65 1.288 151 513.31 1.285 157 510.13 1.277 138 509.16 1.275 107 507.08 1.269 82 505.37 1.265 78 504.03 1.262 67 501.71 1.256 88 369.02 0.924 308 366.82 0.918 217 364.87 0.913 630 362.18 0.907 677 359.74 0.901 178 357.30 0.895 1000 355.10 0.889 375 352.05 0.881 85 349.85 0.876 472
in CDCl3
Liquid film
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