Cinnamyl chloride

Mass

MS-NW-5818          
trans-(3-chloro-1-propenyl)benzene
C9H9Cl              (Mass of molecular ion:    152)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       1.1
      36.0       1.6
      38.0       1.0
      39.0       6.4
      50.0       2.6
      51.0       4.9
      52.0       1.1
      57.0       1.8
      57.5       5.1
      58.0       4.2
      62.0       1.8
      63.0       4.4
      65.0       3.3
      74.0       1.2
      75.0       1.2
      76.0       1.0
      77.0       2.1
      78.0       1.1
      89.0       3.5
      91.0      14.3
      92.0       1.2
     102.0       1.7
     115.0      33.2
     116.0      13.8
     117.0     100.0
     118.0      10.0
     152.0      19.9
     153.0       2.1
     154.0       6.5

Assign. Shift(ppm) A 7.54 to 7.08 B 6.600 C 6.302 D 4.202 J(B,C)=15.6HZ. J(C,D)=6.6HZ.

     Hz     ppm     Int.

    670.09   7.483     30
    669.49   7.476     33
    668.04   7.460     40
    666.85   7.446     32
    666.25   7.440     31
    665.05   7.426     53
    663.09   7.404    108
    662.23   7.395    160
    661.21   7.383    122
    660.10   7.371    113
    658.13   7.349    394
    656.16   7.327   1000
    654.80   7.312    971
    654.20   7.305    900
    653.09   7.293    383
    650.95   7.269    336
    649.41   7.252    226
    648.39   7.240     88
    646.85   7.223    141
    645.65   7.210     67
    645.23   7.205     69
    644.03   7.192     84
    642.66   7.176     37
    641.38   7.162     40
    603.02   6.734    118
    602.33   6.726    150
    586.69   6.551    422
    575.33   6.424    223
    568.66   6.350    342
    562.00   6.276    206
    559.69   6.250     58
    553.03   6.175    121
    546.36   6.101    100
    379.82   4.241    595
    379.05   4.233    623
    373.07   4.166    688