3-Amino-4-chlorobenzotrifluoride
Product Name 3-Amino-4-chlorobenzotrifluoride
CAS121-50-6
MFC7H5ClF3N
MW195.57
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MS-NW-8897 6-chloro-alpha,alpha,alpha-trifluoro-m-toluidine C7H5ClF3N (Mass of molecular ion: 195)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.6 38.0 1.5 39.0 1.5 41.0 1.1 52.0 2.7 57.0 1.1 61.0 1.0 62.0 2.2 63.0 6.0 64.0 1.8 65.0 1.5 69.0 1.1 70.5 1.1 73.0 1.3 75.0 2.1 80.0 7.2 83.0 1.3 88.0 2.4 89.0 1.3 90.0 3.4 91.0 1.2 97.5 1.9 99.0 2.0 109.0 1.3 113.0 4.7 114.0 1.5 120.0 2.4 132.0 6.1 133.0 2.7 139.0 1.5 140.0 9.2 141.0 1.1 145.0 7.1 147.0 3.0 148.0 10.5 149.0 1.0 150.0 3.3 158.0 1.4 159.0 1.3 160.0 13.2 161.0 2.7 167.0 1.3 174.0 1.5 175.0 3.8 176.0 13.2 177.0 2.3 178.0 4.2 194.0 2.3 195.0 100.0 196.0 8.9 197.0 32.5 198.0 2.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H5 Cl F3 N 0.04 ml : 0.5 ml CDCl3 6-chloro-alpha,alpha,alpha-trifluoro-m-toluidine Assign. Shift(ppm)
A 7.32 B 6.956 C 6.93 D 4.21
Hz ppm Int.
659.81 7.368 217 659.00 7.359 159 651.88 7.279 322 651.13 7.271 254 625.81 6.988 112 625.13 6.981 229 624.44 6.973 353 623.75 6.965 670 623.13 6.958 1000 622.44 6.950 787 621.06 6.935 151 620.38 6.927 119 615.88 6.877 83 615.25 6.870 201 614.56 6.862 207 613.88 6.855 128 613.13 6.847 143 612.44 6.839 136 611.75 6.831 60 377.25 4.213 104
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