3-Amino-4-chlorobenzotrifluoride

Mass

MS-NW-8897          
6-chloro-alpha,alpha,alpha-trifluoro-m-toluidine
C7H5ClF3N           (Mass of molecular ion:    195)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       1.6
      38.0       1.5
      39.0       1.5
      41.0       1.1
      52.0       2.7
      57.0       1.1
      61.0       1.0
      62.0       2.2
      63.0       6.0
      64.0       1.8
      65.0       1.5
      69.0       1.1
      70.5       1.1
      73.0       1.3
      75.0       2.1
      80.0       7.2
      83.0       1.3
      88.0       2.4
      89.0       1.3
      90.0       3.4
      91.0       1.2
      97.5       1.9
      99.0       2.0
     109.0       1.3
     113.0       4.7
     114.0       1.5
     120.0       2.4
     132.0       6.1
     133.0       2.7
     139.0       1.5
     140.0       9.2
     141.0       1.1
     145.0       7.1
     147.0       3.0
     148.0      10.5
     149.0       1.0
     150.0       3.3
     158.0       1.4
     159.0       1.3
     160.0      13.2
     161.0       2.7
     167.0       1.3
     174.0       1.5
     175.0       3.8
     176.0      13.2
     177.0       2.3
     178.0       4.2
     194.0       2.3
     195.0     100.0
     196.0       8.9
     197.0      32.5
     198.0       2.6

Assign. Shift(ppm) A 7.32 B 6.956 C 6.93 D 4.21

     Hz     ppm     Int.

    659.81   7.368    217
    659.00   7.359    159
    651.88   7.279    322
    651.13   7.271    254
    625.81   6.988    112
    625.13   6.981    229
    624.44   6.973    353
    623.75   6.965    670
    623.13   6.958   1000
    622.44   6.950    787
    621.06   6.935    151
    620.38   6.927    119
    615.88   6.877     83
    615.25   6.870    201
    614.56   6.862    207
    613.88   6.855    128
    613.13   6.847    143
    612.44   6.839    136
    611.75   6.831     60
    377.25   4.213    104