2,4-Dichlorophenol

Mass

MS-NW-8655          
2,4-dichlorophenol
C6H4Cl2O            (Mass of molecular ion:    162)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      18.0       1.0
      28.0       1.4
      31.0       2.4
      36.0       2.1
      37.0       3.8
      38.0       3.4
      39.0       2.3
      48.0       2.3
      49.0       7.2
      50.0       3.6
      53.0       4.2
      60.0       1.3
      61.0       4.9
      62.0       7.9
      63.0      45.6
      64.0       4.2
      72.0       2.6
      73.0       8.9
      74.0       2.8
      75.0       3.1
      81.0       4.2
      82.0       2.7
      83.0       1.3
      91.0       1.3
      97.0       2.4
      98.0      39.7
      99.0      12.6
     100.0      13.4
     101.0       3.9
     109.0       1.0
     126.0      16.5
     127.0       1.7
     128.0       5.5
     133.0       2.8
     134.0       1.1
     135.0       1.8
     162.0     100.0
     163.0       6.9
     164.0      63.6
     165.0       4.3
     166.0      10.3

Assign. Shift(ppm) A 7.317 B 7.136 C 6.954 D 5.49 J(A,B)=2.5HZ. J(A,C)=0.4HZ. J(B,C)=8.7HZ.

     Hz     ppm     Int.

    656.88   7.335    615
    656.44   7.330    559
    654.50   7.308    906
    654.06   7.304    770
    646.19   7.216    264
    643.88   7.190    134
    637.56   7.119    528
    635.19   7.093    451
    625.56   6.985   1000
    625.13   6.981    898
    616.88   6.888    414
    616.44   6.883    363
    491.81   5.492    828