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MS-NW-8655 2,4-dichlorophenol C6H4Cl2O (Mass of molecular ion: 162)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
18.0 1.0 28.0 1.4 31.0 2.4 36.0 2.1 37.0 3.8 38.0 3.4 39.0 2.3 48.0 2.3 49.0 7.2 50.0 3.6 53.0 4.2 60.0 1.3 61.0 4.9 62.0 7.9 63.0 45.6 64.0 4.2 72.0 2.6 73.0 8.9 74.0 2.8 75.0 3.1 81.0 4.2 82.0 2.7 83.0 1.3 91.0 1.3 97.0 2.4 98.0 39.7 99.0 12.6 100.0 13.4 101.0 3.9 109.0 1.0 126.0 16.5 127.0 1.7 128.0 5.5 133.0 2.8 134.0 1.1 135.0 1.8 162.0 100.0 163.0 6.9 164.0 63.6 165.0 4.3 166.0 10.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H4 Cl2 O 0.046 g : 0.5 ml CDCl3 2,4-dichlorophenol Assign. Shift(ppm)
A 7.317 B 7.136 C 6.954 D 5.49 J(A,B)=2.5HZ. J(A,C)=0.4HZ. J(B,C)=8.7HZ.
Hz ppm Int.
656.88 7.335 615 656.44 7.330 559 654.50 7.308 906 654.06 7.304 770 646.19 7.216 264 643.88 7.190 134 637.56 7.119 528 635.19 7.093 451 625.56 6.985 1000 625.13 6.981 898 616.88 6.888 414 616.44 6.883 363 491.81 5.492 828
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