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Diethyl disulfide

Product Name Diethyl disulfide

CAS110-81-6

MFC4H10S2

MW122.25

¹³CNMR

Mass

MS-NW-3100          
diethyl disulfide
C4H10S2             (Mass of molecular ion:    122)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      26.0       4.5
      27.0      31.6
      28.0       6.2
      29.0      68.5
      30.0       1.5
      32.0       1.2
      34.0       1.2
      35.0       5.6
      45.0       8.6
      46.0       3.0
      47.0       2.9
      57.0       1.2
      58.0       3.8
      59.0       9.7
      60.0      11.0
      61.0       8.5
      62.0       3.0
      64.0       6.4
      65.0       2.5
      66.0      80.9
      67.0       1.6
      68.0       7.3
      76.0       1.6
      79.0       8.4
      89.0       1.1
      93.0       5.2
      94.0      64.0
      95.0       2.9
      96.0       5.6
     122.0     100.0
     123.0       6.1
     124.0       9.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₄ H₁₀ S₂	0.05 ml : 0.5 ml CDCl₃
diethyl disulfide

    Assign.     Shift(ppm)

      A             2.694
      B             1.320

     Hz     ppm     Int.

    253.44   2.830     98
    252.81   2.823     99
    245.63   2.743    410
    238.88   2.668    238
    238.25   2.661    471
    231.44   2.585    142
    230.88   2.578    139
    125.31   1.400    451
    118.19   1.320   1000
    117.75   1.315    652
    110.63   1.236    347

in CDCl3

liquid film

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