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1-Bromopentane

Product Name 1-Bromopentane

CAS110-53-2

MFC5H11Br

MW151.04

¹³CNMR

Mass

MS-NW-2069          
1-bromopentane
C5H11Br             (Mass of molecular ion:    150)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.2
      26.0       2.0
      27.0      18.7
      28.0       2.5
      29.0      22.2
      39.0      10.1
      40.0       1.9
      41.0      33.1
      42.0      30.2
      43.0     100.0
      44.0       3.4
      53.0       1.2
      55.0      27.1
      56.0       1.4
      57.0       1.5
      69.0       1.6
      70.0       5.1
      71.0      84.0
      72.0       4.6
     107.0       1.6
     109.0       1.7
     150.0       3.5
     152.0       3.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₁ Br	0.04 ml : 0.5 ml CDCl₃
1-bromopentane

    Assign.     Shift(ppm)

      A             3.398
      B             1.86
      C             1.44
      D             1.32
      E             0.93

     Hz     ppm     Int.

    311.63   3.480    392
    304.94   3.405   1000
    302.38   3.377     35
    298.13   3.329    552
    296.56   3.312     37
    181.94   2.032     31
    180.69   2.018     37
    176.50   1.971     51
    175.69   1.962     70
    173.94   1.943    120
    172.75   1.929     89
    171.50   1.915     77
    170.13   1.900     92
    169.50   1.893     87
    167.31   1.869    176
    166.38   1.858    153
    164.13   1.833     88
    163.31   1.824     85
    161.88   1.808     88
    160.63   1.794    140
    159.94   1.786    148
    157.94   1.764     62
    156.38   1.747     43
    156.00   1.742     42
    154.88   1.730     47
    153.63   1.716     67
    151.94   1.697     31
    141.63   1.582     33
    140.50   1.569     48
    139.19   1.555     31
    138.13   1.543     43
    136.00   1.519     57
    134.50   1.502     78
    132.63   1.481    183
    129.25   1.444    229
    127.63   1.426    207
    126.44   1.412    225
    125.38   1.400    395
    124.50   1.391    333
    122.56   1.369    247
    121.69   1.359    294
    121.19   1.354    267
    120.31   1.344    218
    119.25   1.332    157
    117.88   1.317    364
    115.50   1.290    114
    114.44   1.278    112
    113.19   1.264     68
    112.25   1.254     74
    110.38   1.233     63
    109.44   1.222     70
    108.50   1.212     52
    105.63   1.180     33
    103.63   1.158     40
    101.75   1.137     33
     93.81   1.048     30
     93.38   1.043     30
     92.81   1.037     35
     92.06   1.028     44
     91.38   1.021     46
     90.50   1.011     56
     89.31   0.998    161
     88.38   0.987    258
     87.56   0.978    250
     86.44   0.966    140
     85.63   0.957    139
     85.00   0.950    132
     84.00   0.938    184
     81.94   0.915    682
     79.56   0.889    148
     78.81   0.880    141
     76.56   0.855    123
     76.00   0.849    127
     74.56   0.833    105
     74.06   0.827     89
     72.56   0.811     58
     72.00   0.804     52

in CDCl3

CCl4 solution

liquid film

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