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3-Dimethylaminopropylamine

Product Name 3-Dimethylaminopropylamine

CAS109-55-7

MFC5H14N2

MW102.18

¹³CNMR

Mass

MS-NW-0595          
N,N-dimethyltrimethylenediamine
C5H14N2             (Mass of molecular ion:    102)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       3.3
      17.0       1.5
      18.0       7.8
      27.0       1.6
      28.0       5.2
      29.0       2.0
      30.0      15.7
      41.0       2.4
      42.0      11.5
      43.0       4.7
      44.0      11.4
      45.0       2.5
      46.0       4.8
      56.0       5.9
      57.0       6.2
      58.0     100.0
      59.0       4.9
      70.0       3.9
      71.0       1.5
      72.0       6.2
      84.0       2.5
      85.0      20.4
      86.0       1.2
     102.0       2.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₄ N₂	0.05 ml : 0.5 ml CDCl₃
N,N-dimethyltrimethylenediamine

    Assign.     Shift(ppm)

      A             2.745
      B             2.25
      C             2.216
      D             1.60
      E             1.15

     Hz     ppm     Int.

    252.63   2.821     56
    245.75   2.744    123
    238.88   2.668     74
    215.00   2.401     46
    214.31   2.393     46
    207.88   2.322     97
    204.75   2.287     34
    198.56   2.218   1000
    150.69   1.683     43
    150.00   1.675     48
    143.31   1.601     59
    136.63   1.526     30
    135.88   1.518     34
    103.00   1.151    140

in CDCl3

liquid film

4880 A,100M,liquid

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