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N-[2-(4-Bromophenoxy)ethyl]pyrrolidine

Product Name N-[2-(4-Bromophenoxy)ethyl]pyrrolidine

CAS1081-73-8

MFC12H16BrNO

MW270.17


  • Mass 

    MS-IW-1309          
1-(2-(p-bromophenoxy)ethyl)pyrrolidine
C12H16BrNO          (Mass of molecular ion:    269)


       Source Temperature: 230 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV


          28.0       1.0
      30.0       1.2
      41.0       2.0
      42.0       6.6
      55.0       3.5
      56.0       2.9
      69.0       1.4
      82.0       1.3
      84.0     100.0
      85.0       6.1
      96.0       1.2
      97.0       1.2
      98.0       1.1
     269.0       1.5
     271.0       1.4

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H16 Br N O 0.05 ml : 0.5 ml CDCl3
    1-(2-(p-bromophenoxy)ethyl)pyrrolidine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.335
      B             6.783
      C             4.042
      D             2.866
      E             2.60
      F             1.783
  

         Hz     ppm     Int.


        665.56   7.432     83
    664.75   7.423     57
    662.31   7.396    684
    660.00   7.370    244
    658.31   7.351     71
    657.75   7.345     75
    655.50   7.320    290
    653.19   7.294   1000
    649.94   7.258    135
    614.75   6.865    113
    611.50   6.828    858
    609.19   6.803    259
    604.63   6.752    222
    602.38   6.726    611
    599.19   6.691     81
    368.31   4.113    361
    365.94   4.086     73
    362.38   4.047    806
    359.69   4.017     71
    356.50   3.981    442
    262.31   2.929    453
    260.19   2.906     80
    256.50   2.865    825
    253.25   2.828     91
    250.50   2.798    378
    246.50   2.753     49
    245.94   2.747     48
    245.56   2.742     48
    243.88   2.724     59
    243.00   2.714     62
    242.13   2.704     67
    239.94   2.680    184
    239.13   2.671    222
    237.75   2.655    253
    237.00   2.647    251
    235.44   2.629    323
    232.75   2.599    670
    230.63   2.576    468
    228.81   2.555    333
    227.25   2.538    345
    226.13   2.525    372
    223.44   2.495    117
    219.81   2.455     61
    174.56   1.950     44
    169.50   1.893     74
    166.50   1.860    314
    163.44   1.825    405
    159.75   1.784    782
    156.25   1.745    423
    153.19   1.711    260
    150.31   1.679     83

in CDCl3



liquid film



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