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3,5-Dimethylaniline

Product Name 3,5-Dimethylaniline

CAS108-69-0

MFC8H11N

MW121.18

¹³CNMR

Mass

MS-NW-0576          
3,5-xylidine
C8H11N              (Mass of molecular ion:    121)

   Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       1.1
      27.0       2.5
      28.0       3.0
      38.0       1.2
      39.0       5.0
      41.0       2.6
      42.0       2.7
      50.0       1.4
      51.0       3.7
      52.0       2.5
      53.0       3.6
      54.0       1.4
      58.5       1.5
      59.5       1.7
      60.5       1.1
      63.0       1.5
      65.0       3.1
      66.0       1.5
      77.0      10.6
      78.0       3.5
      79.0       5.3
      80.0       2.5
      91.0       5.9
      92.0       1.3
      93.0       4.1
      94.0       1.6
     103.0       2.5
     104.0       2.5
     105.0       2.6
     106.0      41.6
     107.0       3.4
     118.0       1.8
     119.0       1.5
     120.0      37.9
     121.0     100.0
     122.0       9.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₁ N	0.04 ml : 0.5 ml CDCl₃
3,5-xylidine

    Assign.     Shift(ppm)

      A             6.40
      B             6.30
      C             3.46
      D             2.207

     Hz     ppm     Int.

    573.31   6.402     76
    572.63   6.394     77
    572.00   6.387     65
    571.31   6.380     44
    565.25   6.312    132
    564.69   6.306    182
    564.06   6.299    182
    563.31   6.290    153
    310.00   3.462    454
    198.06   2.212   1000
    197.44   2.205    959

in CDCl3

liquid film

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