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3,5-Dimethylaniline

Product Name 3,5-Dimethylaniline

CAS108-69-0

MFC8H11N

MW121.18

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  • Mass 

    MS-NW-0576          
3,5-xylidine
C8H11N              (Mass of molecular ion:    121)


       Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV


          18.0       1.1
      27.0       2.5
      28.0       3.0
      38.0       1.2
      39.0       5.0
      41.0       2.6
      42.0       2.7
      50.0       1.4
      51.0       3.7
      52.0       2.5
      53.0       3.6
      54.0       1.4
      58.5       1.5
      59.5       1.7
      60.5       1.1
      63.0       1.5
      65.0       3.1
      66.0       1.5
      77.0      10.6
      78.0       3.5
      79.0       5.3
      80.0       2.5
      91.0       5.9
      92.0       1.3
      93.0       4.1
      94.0       1.6
     103.0       2.5
     104.0       2.5
     105.0       2.6
     106.0      41.6
     107.0       3.4
     118.0       1.8
     119.0       1.5
     120.0      37.9
     121.0     100.0
     122.0       9.4

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H11 N 0.04 ml : 0.5 ml CDCl3
    3,5-xylidine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.40
      B             6.30
      C             3.46
      D             2.207
  

         Hz     ppm     Int.


        573.31   6.402     76
    572.63   6.394     77
    572.00   6.387     65
    571.31   6.380     44
    565.25   6.312    132
    564.69   6.306    182
    564.06   6.299    182
    563.31   6.290    153
    310.00   3.462    454
    198.06   2.212   1000
    197.44   2.205    959

in CDCl3



liquid film





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