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Diisopropylamine

Product Name Diisopropylamine

CAS108-18-9

MFC6H15N

MW101.19

¹³CNMR

Mass

MS-NW-0580          
diisopropylamine
C6H15N              (Mass of molecular ion:    101)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       2.7
      18.0       3.3
      27.0       5.4
      28.0       4.5
      30.0       1.8
      39.0       3.4
      41.0       8.1
      42.0       9.2
      43.0       9.2
      44.0     100.0
      45.0       2.6
      56.0       1.6
      58.0       8.1
      70.0       2.0
      86.0      41.8
      87.0       2.4
     100.0       1.3
     101.0       3.8

90 MHz in CDCl3

parameter neat

¹H NMR	89.56 MHz
C₆ H₁₅ N	0.04 ml : 0.5 ml CDCl₃
diisopropylamine

    Assign.     Shift(ppm)

      A             2.91
      B             1.042
      C             1.0

     Hz     ppm     Int.

    266.88   2.980     47
    260.63   2.911     63
    254.38   2.841     52
    248.19   2.772     24
     96.31   1.076   1000
     92.75   1.036     35
     90.06   1.006    907

¹H NMR	300 MHz
C₆ H₁₅ N	neat
diisopropylamine

    Parameter     ppm  Hz

      D(A)         2.86
      D(B)         1.00
       J(A,B)          6.3
     
      D(C)         3.06
     
     RANFT,J. ANN.PHYS. 10, 1 (1962)

     Hz     ppm     Int.

    918.00   3.060    166
    870.71   2.902     29
    864.40   2.881     72
    858.09   2.860     98
    851.80   2.839     76
    845.51   2.818     32
    303.14   1.010   1000
    296.85   0.989    974

in CDCl3