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MS-NW-1132 1-vinylimidazole C5H6N2 (Mass of molecular ion: 94)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.5 18.0 1.1 26.0 7.5 27.0 16.6 28.0 12.9 37.0 1.4 38.0 3.4 39.0 13.8 40.0 28.6 41.0 52.6 42.0 3.7 51.0 1.5 52.0 4.6 53.0 1.7 54.0 3.3 66.0 3.2 67.0 26.1 68.0 5.3 79.0 1.3 93.0 3.1 94.0 100.0 95.0 6.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H6 N2 0.02 ml : 0.5 ml CDCl3 1-vinylimidazole Assign. Shift(ppm)
A 7.644 B 7.173 C 7.083 D 6.894 E 5.274 F 4.871
Hz ppm Int.
684.63 7.645 668 643.63 7.187 498 642.50 7.174 1000 641.19 7.160 634 639.19 7.138 78 634.25 7.082 800 630.31 7.038 373 621.50 6.940 369 614.56 6.862 405 605.81 6.765 443 480.25 5.363 694 478.56 5.344 719 464.50 5.187 548 462.81 5.168 599 441.25 4.927 445 439.56 4.908 424 432.38 4.828 414 430.81 4.811 373
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