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MassMS-NW-1111 1-chloro-3-methylbutane C5H11Cl (Mass of molecular ion: 106)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.4 26.0 2.0 27.0 21.3 28.0 4.6 29.0 19.1 32.0 1.0 38.0 1.4 39.0 14.0 40.0 2.0 41.0 39.2 42.0 35.5 43.0 100.0 44.0 3.4 49.0 1.7 50.0 1.0 51.0 1.5 53.0 3.5 54.0 1.1 55.0 50.9 56.0 7.1 57.0 14.1 59.0 1.2 62.0 1.0 63.0 4.1 65.0 1.3 69.0 6.4 70.0 49.8 71.0 10.3 76.0 4.1 77.0 7.5 78.0 1.5 79.0 2.5 83.0 1.6 84.0 1.5 85.0 1.4 90.0 1.1 91.0 4.7 93.0 1.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 Cl 0.04 ml : 0.5 ml CDCl3 1-chloro-3-methylbutane 
Assign. Shift(ppm)
A 3.553 B 2.02 to 1.41 C 0.925
Hz ppm Int.325.19 3.631 214 318.38 3.555 363 311.56 3.479 218 157.44 1.758 118 155.94 1.742 102 155.44 1.736 110 151.25 1.689 191 148.81 1.662 102 145.38 1.624 132 144.31 1.612 161 139.75 1.561 398 85.50 0.955 1000 83.06 0.928 136 82.75 0.924 133 82.31 0.920 129 79.56 0.889 825
in CDCl3
CCl4 solution
liquid film
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