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p-Phenylenediamine

Product Name p-Phenylenediamine

CAS106-50-3

MFC6H8N2

MW108.14

¹³CNMR

Mass

MS-NW-8710          
p-phenylenediamine
C6H8N2              (Mass of molecular ion:    108)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.1
      27.0       2.0
      28.0       5.5
      38.0       1.0
      39.0       2.9
      40.0       2.1
      41.0       3.3
      42.0       1.4
      51.0       2.3
      52.0       7.7
      53.0      12.1
      53.5       1.9
      54.0      13.1
      55.0       2.1
      63.0       2.2
      64.0       2.4
      65.0       2.3
      66.0       1.3
      67.0       2.8
      78.0       1.3
      79.0       1.9
      80.0      33.2
      81.0      15.9
      82.0       1.6
      90.0       1.4
      91.0       3.2
     105.0       1.0
     106.0       1.1
     107.0      24.5
     108.0     100.0
     109.0       7.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₈ N₂	0.048 g : 0.5 ml CDCl₃
p-phenylenediamine

    Assign.     Shift(ppm)

      A             6.557
      B             3.3

     Hz     ppm     Int.

    587.25   6.558   1000
    296.00   3.306     41

in CDCl3

KBr disc

nujol mull

CATION RADICAL, ELECTROXID., PH=4.8

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