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Ethylene glycol diphenyl ether

Product Name Ethylene glycol diphenyl ether

CAS104-66-5

MFC14H14O2

MW214.26

¹³CNMR

Mass

MS-NW-2384          
ethylene glycol diphenyl ether
C14H14O2            (Mass of molecular ion:    214)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       3.0
      27.0       2.5
      38.0       2.5
      39.0      16.7
      40.0       1.6
      43.0       3.6
      50.0       3.0
      51.0      16.4
      52.0       1.1
      55.0       1.6
      63.0       3.7
      64.0       1.9
      65.0      24.7
      66.0       4.6
      76.0       1.3
      77.0     100.0
      78.0       7.8
      79.0       5.8
      91.0      19.6
      92.0       4.6
      93.0      20.8
      94.0      16.5
      95.0       1.5
     103.0       6.6
     107.0      11.6
     119.0       5.6
     120.0      49.4
     121.0      83.2
     122.0       7.2
     141.0       1.0
     214.0      61.1
     215.0       9.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₄ H₁₄ O₂	0.051 g : 0.5 ml CDCl₃
ethylene glycol diphenyl ether

    Assign.     Shift(ppm)

      A             7.26
      B          7.05 to 6.83
      C             4.286

     Hz     ppm     Int.

    661.06   7.382     43
    660.06   7.371     68
    658.06   7.348     39
    654.75   7.311     38
    653.69   7.299     92
    652.56   7.287    115
    651.75   7.278     84
    651.06   7.270     84
    650.25   7.261     42
    649.63   7.254     47
    649.13   7.248     42
    645.13   7.204    146
    644.38   7.195    169
    642.25   7.172     34
    629.75   7.032     39
    628.81   7.022     74
    628.13   7.014    117
    627.44   7.006     75
    626.75   6.999     45
    625.50   6.985    203
    624.50   6.973    230
    623.44   6.962     91
    622.13   6.947    136
    621.44   6.939    116
    619.00   6.912     63
    618.44   6.906     66
    617.06   6.890    135
    616.38   6.883    106
    615.81   6.876    135
    614.56   6.862     54
    613.31   6.849     31
    383.88   4.287   1000

in CDCl3

CCl4 solution

KBr disc

nujol mull

4880 A,200 M,powder

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