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MS-NW-2384 ethylene glycol diphenyl ether C14H14O2 (Mass of molecular ion: 214)
Source Temperature: 280 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 3.0 27.0 2.5 38.0 2.5 39.0 16.7 40.0 1.6 43.0 3.6 50.0 3.0 51.0 16.4 52.0 1.1 55.0 1.6 63.0 3.7 64.0 1.9 65.0 24.7 66.0 4.6 76.0 1.3 77.0 100.0 78.0 7.8 79.0 5.8 91.0 19.6 92.0 4.6 93.0 20.8 94.0 16.5 95.0 1.5 103.0 6.6 107.0 11.6 119.0 5.6 120.0 49.4 121.0 83.2 122.0 7.2 141.0 1.0 214.0 61.1 215.0 9.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H14 O2 0.051 g : 0.5 ml CDCl3 ethylene glycol diphenyl ether Assign. Shift(ppm)
A 7.26 B 7.05 to 6.83 C 4.286
Hz ppm Int.
661.06 7.382 43 660.06 7.371 68 658.06 7.348 39 654.75 7.311 38 653.69 7.299 92 652.56 7.287 115 651.75 7.278 84 651.06 7.270 84 650.25 7.261 42 649.63 7.254 47 649.13 7.248 42 645.13 7.204 146 644.38 7.195 169 642.25 7.172 34 629.75 7.032 39 628.81 7.022 74 628.13 7.014 117 627.44 7.006 75 626.75 6.999 45 625.50 6.985 203 624.50 6.973 230 623.44 6.962 91 622.13 6.947 136 621.44 6.939 116 619.00 6.912 63 618.44 6.906 66 617.06 6.890 135 616.38 6.883 106 615.81 6.876 135 614.56 6.862 54 613.31 6.849 31 383.88 4.287 1000
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