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MS-NW-8367 phenethyl bromide C8H9Br (Mass of molecular ion: 184)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
27.0 3.9 38.0 1.2 39.0 5.3 50.0 5.0 51.0 12.9 52.0 2.9 62.0 1.2 63.0 3.3 65.0 6.1 74.0 1.7 75.0 1.3 76.0 1.5 77.0 13.9 78.0 6.7 79.0 9.5 89.0 1.6 91.0 100.0 92.0 7.7 102.0 1.4 103.0 8.2 104.0 8.1 105.0 63.0 106.0 5.6 184.0 19.1 185.0 1.7 186.0 18.6 187.0 1.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 Br 0.04 ml : 0.5 ml CDCl3 phenethyl bromide Assign. Shift(ppm)
A 7.34 to 7.15 B 3.535 C 3.154
Hz ppm Int.
658.56 7.354 112 656.50 7.331 98 655.00 7.314 141 652.06 7.281 390 650.00 7.258 1000 647.50 7.230 978 645.19 7.204 314 643.06 7.181 226 640.69 7.154 97 640.31 7.150 93 638.88 7.134 113 326.56 3.647 211 324.81 3.627 244 319.63 3.569 270 318.13 3.553 436 317.69 3.548 494 317.13 3.541 421 311.25 3.476 508 310.31 3.465 509 288.56 3.222 359 287.94 3.216 353 281.25 3.141 394 279.44 3.121 206 274.19 3.062 143 272.44 3.042 137
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